John Jacob Livingood made radium E (210Bi) by bombarding common bismuth with deuterons, 1936, the first synthetis of a radioactive substance in the US.
Lydia Sesemann born 1845: first woman to receive a doctorate in chemistry from the University of Zürich and probably the first woman in the world to receive a doctorate in chemistry
Ernest Marsden born 1889: scattering of alpha particles (work with Hans Geiger in Ernest Rutherford's lab), contributing to the development of the nuclear model of the atom. (Read 1909 and 1913 papers with Geiger.)
Pierre Jules Cesar Janssen born 1824: astronomical spectroscopy and photography, particularly of the Sun; found a line in the solar spectrum subsequently identified with helium.